The Democratic Alliance held its final campaign rally at a vast events centre in Johannesburg's upmarket suburb of Northriding.
"The ANC has become arrogant because they believe that the voters will carry on voting for them, whatever they do," said leader Helen Zille.
"Well, they are in for a big shock on Wednesday."
South Africans go to the polls on May 7 to elect provincial leaders and legislators. The lawmakers will then elect a president from the party which garners the most number of votes.
Switching between English, Xhosa, Afrikaans and at times throwing in slogans in Sotho, Zille said her party was the "only hope for positive change" in South Africa.
She hit out at President Jacob Zuma, contrasting his leadership with that of fellow ANC leaders Nelson Mandela and Thabo Mbeki, who she said stewarded the country toward economic growth and development.
Zille claimed that during the last five years under Zuma, unemployment has climbed and conditions had deteriorated for the country's poor majority because the ANC's current crop of leaders "believe they will rule forever."
"It is not the organisation it once was."
"When a government becomes corrupt, when it does not do its job properly, the economy declines, unemployment grows, poverty deepens and the powerful few get richer and richer."
"That is the sad story of our own country over the last five years," she said.
"We demand change -- less corruption, better services and more jobs," she said to wild applause from a sea of supporters in blue at the 18,000-seater Coca Cola Dome.
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